Information card for entry 7024138

Structure parameters

• Common name: (K(2,2,2-crypt))4(Cd(P7)2)*6py
• Chemical name: [K(2,2,2-crypt)]4[Cd(P7)2]*6py
• Formula: C102 H174 Cd K4 N14 O24 P14
• Calculated formula: C102 H174 Cd K4 N14 O24 P14
• Title of publication: Reactivity studies of group 15 Zintl ions towards homoleptic post-transition metal organometallics: a 'bottom-up' approach to bimetallic molecular clusters.
• Authors of publication: Knapp, Caroline; Zhou, Binbin; Denning, Mark S.; Rees, Nicholas H.; Goicoechea, Jose M.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 2
• Pages of publication: 426 - 436
• a: 23.5977 ± 0.0002 Å
• b: 75.1887 ± 0.0008 Å
• c: 15.1082 ± 0.0001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 26806.2 ± 0.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 43
• Hermann-Mauguin space group symbol: F d d 2
• Hall space group symbol: F 2 -2d
• Residual factor for all reflections: 0.0769
• Residual factor for significantly intense reflections: 0.0541
• Weighted residual factors for significantly intense reflections: 0.1086
• Weighted residual factors for all reflections included in the refinement: 0.1161
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No