Information card for entry 7024158

Structure parameters

• Formula: C53 H24 F72 K8 O8
• Calculated formula: C53 H24 F72 K8 O8
• Title of publication: Three-coordinate late transition metal fluorinated alkoxide complexes.
• Authors of publication: Cantalupo, Stefanie A.; Lum, June S.; Buzzeo, Marisa C.; Moore, Curtis; DiPasquale, Antonio G.; Rheingold, Arnold L.; Doerrer, Linda H.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 2
• Pages of publication: 374 - 383
• a: 21.061 ± 0.011 Å
• b: 21.046 ± 0.011 Å
• c: 21.082 ± 0.01 Å
• α: 90°
• β: 113.734 ± 0.006°
• γ: 90°
• Cell volume: 8554 ± 8 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0679
• Residual factor for significantly intense reflections: 0.0396
• Weighted residual factors for significantly intense reflections: 0.0852
• Weighted residual factors for all reflections included in the refinement: 0.1002
• Goodness-of-fit parameter for all reflections included in the refinement: 1.038
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No