Information card for entry 7024211

Structure parameters

• Formula: C39 H33 Cl4 N2 P Zn
• Calculated formula: C39 H33 Cl4 N2 P Zn
• Title of publication: Electron rich bidentate phosphinimine-imine ligands: synthesis and reactivity of late transition metal complexes.
• Authors of publication: Wallis, Christopher J.; Kraft, Ira L.; Patrick, Brian O.; Mehrkhodavandi, Parisa
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 2
• Pages of publication: 541 - 547
• a: 12.364 ± 0.0009 Å
• b: 17.4916 ± 0.0014 Å
• c: 16.9571 ± 0.0013 Å
• α: 90°
• β: 99.222 ± 0.003°
• γ: 90°
• Cell volume: 3619.8 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0468
• Residual factor for significantly intense reflections: 0.0313
• Weighted residual factors for significantly intense reflections: 0.0738
• Weighted residual factors for all reflections included in the refinement: 0.0806
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No