Information card for entry 7024298

Structure parameters

• Formula: C32 H25 Cl2 F N P Pd
• Calculated formula: C32 H25 Cl2 F N P Pd
• Title of publication: Synthesis and reactivity of palladium(II) fluoride complexes containing nitrogen-donor ligands.
• Authors of publication: Ball, Nicholas D.; Kampf, Jeff W.; Sanford, Melanie S.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 2
• Pages of publication: 632 - 640
• a: 8.7399 ± 0.0005 Å
• b: 17.2959 ± 0.0009 Å
• c: 20.3468 ± 0.0011 Å
• α: 96.861 ± 0.001°
• β: 98.293 ± 0.001°
• γ: 104.123 ± 0.001°
• Cell volume: 2913 ± 0.3 ų
• Cell temperature: 85 ± 2 K
• Ambient diffraction temperature: 85 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0403
• Residual factor for significantly intense reflections: 0.0367
• Weighted residual factors for significantly intense reflections: 0.0934
• Weighted residual factors for all reflections included in the refinement: 0.0961
• Goodness-of-fit parameter for all reflections included in the refinement: 1.055
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No