Information card for entry 7024354

Structure parameters

• Formula: C36 H24 N18 Ni3 O4
• Calculated formula: C36 H24 N18 Ni3 O4
• Title of publication: One-dimensional metal-azido complex constructed by a double EO azido bridged trinuclear nickel(II) unit: synthesis, structure and magnetic properties.
• Authors of publication: Liu, Fu-Chen; Zhao, Jiong-Peng; Hu, Bo-Wen; Zeng, Yong-Fei; Ribas, J.; Bu, Xian-He
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 5
• Pages of publication: 1185 - 1187
• a: 11.8807 ± 0.0017 Å
• b: 9.914 ± 0.0014 Å
• c: 17.161 ± 0.003 Å
• α: 90°
• β: 108.588 ± 0.002°
• γ: 90°
• Cell volume: 1915.9 ± 0.5 ų
• Cell temperature: 294 ± 2 K
• Ambient diffraction temperature: 294 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0465
• Residual factor for significantly intense reflections: 0.0303
• Weighted residual factors for significantly intense reflections: 0.0605
• Weighted residual factors for all reflections included in the refinement: 0.0671
• Goodness-of-fit parameter for all reflections included in the refinement: 1.043
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No