Information card for entry 7024382

Structure parameters

• Common name: Tetrafluorobis(1,2-bis(isopropylthio)ethane-S,S')niobium(V) hexafluoroniobate(V)
• Chemical name: Tetrafluorobis(1,2-bis(isopropylthio)ethane-S,S')niobium(V) hexafluoroniobate(V)
• Formula: C16 H36 F10 Nb2 S4
• Calculated formula: C16 H36 F10 Nb2 S4
• Title of publication: Six- and eight-coordinate thio- and seleno-ether complexes of NbF5 and some comparisons with NbCl5 and NbBr5 adducts.
• Authors of publication: Jura, Marek; Levason, William; Ratnani, Raju; Reid, Gillian; Webster, Michael
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 3
• Pages of publication: 883 - 891
• a: 10.285 ± 0.001 Å
• b: 11.6895 ± 0.0015 Å
• c: 13.5404 ± 0.0015 Å
• α: 115.206 ± 0.007°
• β: 90.596 ± 0.01°
• γ: 110.136 ± 0.01°
• Cell volume: 1359.1 ± 0.3 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0655
• Residual factor for significantly intense reflections: 0.047
• Weighted residual factors for significantly intense reflections: 0.1021
• Weighted residual factors for all reflections included in the refinement: 0.1128
• Goodness-of-fit parameter for all reflections included in the refinement: 1.111
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No