Information card for entry 7024400

Structure parameters

• Formula: C27 H46 Cl12 N12 Pd
• Calculated formula: C27 H46 Cl12 N12 Pd
• Title of publication: Coordination of neutral, methylene bridged bis-guanidyls at palladium.
• Authors of publication: Khalaf, Majid S.; Oakley, Sarah H.; Coles, Martyn P.; Hitchcock, Peter B.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 6
• Pages of publication: 1635 - 1642
• a: 11.2121 ± 0.0003 Å
• b: 17.9696 ± 0.0007 Å
• c: 22.7166 ± 0.0008 Å
• α: 90°
• β: 96.199 ± 0.002°
• γ: 90°
• Cell volume: 4550.1 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0791
• Residual factor for significantly intense reflections: 0.0496
• Weighted residual factors for significantly intense reflections: 0.1223
• Weighted residual factors for all reflections included in the refinement: 0.1452
• Goodness-of-fit parameter for all reflections included in the refinement: 1.088
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No