Information card for entry 7024425

Structure parameters

• Chemical name: tetrakis(bis(2-pyridylmethyl)tert-butylamine) bis(?-carbonato) tetranickel perchlorate
• Formula: C39 H60 Cl2 N6 Ni2 O14
• Calculated formula: C39 H60 Cl2 N6 Ni2 O14
• Title of publication: Carbonate formation within a nickel dimer: synthesis of a coordinatively unsaturated bis(mu-hydroxo) dinickel complex and its reactivity toward carbon dioxide.
• Authors of publication: Wikstrom, Jeffrey P.; Filatov, Alexander S.; Mikhalyova, Elena A.; Shatruk, Michael; Foxman, Bruce M.; Rybak-Akimova, Elena V
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 10
• Pages of publication: 2504 - 2514
• a: 12.688 ± 0.0014 Å
• b: 14.1872 ± 0.0015 Å
• c: 15.4415 ± 0.0017 Å
• α: 68.135 ± 0.002°
• β: 67.785 ± 0.002°
• γ: 68.303 ± 0.002°
• Cell volume: 2301.8 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0695
• Residual factor for significantly intense reflections: 0.052
• Weighted residual factors for significantly intense reflections: 0.1295
• Weighted residual factors for all reflections included in the refinement: 0.1507
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: Mo-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No