Information card for entry 7024435

Structure parameters

• Formula: C27.66 H29.32 Cl2 N2 O5 P2 Pd
• Calculated formula: C27.658 H24 Cl2 N2 O5 P2 Pd
• Title of publication: Synthesis of 1,3-azaphosphol-2-ones. Crystal and molecular structures of [SP-4-2]-dichlorobis(3-phenyl-1,3-dihydrobenzo[1,3]azaphosphol-2-one-P)palladium(II) and its chloro(methyl)platinum(II) analogue.
• Authors of publication: Bennett, Justine; Doyle, Roy J.; Lee, Hwi-Young; Lu, Di; Salem, Geoffrey; Speldewinde, David J.; Tifan, Michelle; Willis, Anthony C.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 1
• Pages of publication: 256 - 264
• a: 8.6093 ± 0.0002 Å
• b: 11.3301 ± 0.0003 Å
• c: 16.3435 ± 0.0005 Å
• α: 81.4299 ± 0.0012°
• β: 83.0012 ± 0.0016°
• γ: 77.0439 ± 0.0016°
• Cell volume: 1529.8 ± 0.07 ų
• Cell temperature: 200 K
• Ambient diffraction temperature: 200 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0489
• Residual factor for significantly intense reflections: 0.0284
• Weighted residual factors for all reflections: 0.0411
• Weighted residual factors for significantly intense reflections: 0.0334
• Weighted residual factors for all reflections included in the refinement: 0.0334
• Goodness-of-fit parameter for all reflections included in the refinement: 1.1131
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No