Information card for entry 7024576

Structure parameters

• Formula: C6 H28 Mo12 N4 Ni O44 P Sb2
• Calculated formula: C6 H20 Mo12 N4 Ni O44 P Sb2
• Title of publication: First examples of extended structures based on {PMo(12)Sb(2)O(40)} polyoxoanions.
• Authors of publication: Shi, Shu-Yun; Sun, Ying-Hua; Chen, Yan; Xu, Jia-Ning; Cui, Xiao-Bing; Wang, Yan; Wang, Guo-Wu; Yang, Guang-Di; Xu, Ji-Qing
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 5
• Pages of publication: 1389 - 1394
• a: 9.791 ± 0.002 Å
• b: 10.617 ± 0.002 Å
• c: 11.905 ± 0.002 Å
• α: 79.31 ± 0.03°
• β: 79.82 ± 0.03°
• γ: 68.59 ± 0.03°
• Cell volume: 1124.1 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0377
• Residual factor for significantly intense reflections: 0.0333
• Weighted residual factors for significantly intense reflections: 0.0854
• Weighted residual factors for all reflections included in the refinement: 0.0882
• Goodness-of-fit parameter for all reflections included in the refinement: 1.081
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No