Information card for entry 7024627

Structure parameters

• Formula: C30 H37 N6 Ni O46 P W12
• Calculated formula: C30 H24 N6 Ni O46 P W12
• Title of publication: Hydrothermal syntheses and characterizations of two novel frameworks constructed from polyoxometalates, metals and organic units.
• Authors of publication: Wang, Yan; Ye, Ling; Wang, Tie-Gang; Cui, Xiao-Bing; Shi, Shu-Yun; Wang, Guo-Wu; Xu, Ji-Qing
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 8
• Pages of publication: 1916 - 1919
• a: 24.241 ± 0.005 Å
• b: 11.25 ± 0.002 Å
• c: 28.261 ± 0.006 Å
• α: 90°
• β: 115.06 ± 0.03°
• γ: 90°
• Cell volume: 6982 ± 3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0844
• Residual factor for significantly intense reflections: 0.0664
• Weighted residual factors for significantly intense reflections: 0.1571
• Weighted residual factors for all reflections included in the refinement: 0.1674
• Goodness-of-fit parameter for all reflections included in the refinement: 1.084
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No