Information card for entry 7024669

Structure parameters

• Formula: C47.75 H55.75 Al2 Cl8.25 N3
• Calculated formula: C47 H55 Al2 Cl6 N3
• Title of publication: Disproportionation and radical formation in the coordination of "GaI" with bis(imino)pyridines.
• Authors of publication: Jurca, Titel; Dawson, Karl; Mallov, Ian; Burchell, Tara; Yap, Glenn P. A.; Richeson, Darrin S.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 5
• Pages of publication: 1266 - 1272
• a: 15.124 ± 0.004 Å
• b: 18.054 ± 0.005 Å
• c: 22.939 ± 0.006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6263 ± 3 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 5
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.0923
• Residual factor for significantly intense reflections: 0.0657
• Weighted residual factors for significantly intense reflections: 0.1869
• Weighted residual factors for all reflections included in the refinement: 0.2066
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No