New discrete and polymeric supramolecular architectures derived from dinuclear Co(II), Ni(II) and Cu(II) complexes of aryl-linked bis-beta-diketonato ligands and nitrogen bases: synthetic, structural and high pressure studies.
Authors of publication
Clegg, Jack K.; Hayter, Michael J.; Jolliffe, Katrina A.; Lindoy, Leonard F.; McMurtrie, John C.; Meehan, George V.; Neville, Suzanne M.; Parsons, Simon; Tasker, Peter A.; Turner, Peter; White, Fraser J.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2010
Journal volume
39
Journal issue
11
Pages of publication
2804 - 2815
a
29.6686 ± 0.0016 Å
b
10.3395 ± 0.0007 Å
c
19.7231 ± 0.001 Å
α
90°
β
114.835 ± 0.003°
γ
90°
Cell volume
5490.7 ± 0.6 Å3
Cell temperature
150 ± 2 K
Ambient diffraction temperature
150 ± 2 K
Number of distinct elements
5
Space group number
15
Hermann-Mauguin space group symbol
C 1 2/c 1
Hall space group symbol
-C 2yc
Residual factor for all reflections
0.119
Residual factor for significantly intense reflections
0.0532
Weighted residual factors for significantly intense reflections
0.1101
Weighted residual factors for all reflections included in the refinement
0.1343
Goodness-of-fit parameter for all reflections included in the refinement
