New discrete and polymeric supramolecular architectures derived from dinuclear Co(II), Ni(II) and Cu(II) complexes of aryl-linked bis-beta-diketonato ligands and nitrogen bases: synthetic, structural and high pressure studies.
Authors of publication
Clegg, Jack K.; Hayter, Michael J.; Jolliffe, Katrina A.; Lindoy, Leonard F.; McMurtrie, John C.; Meehan, George V.; Neville, Suzanne M.; Parsons, Simon; Tasker, Peter A.; Turner, Peter; White, Fraser J.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2010
Journal volume
39
Journal issue
11
Pages of publication
2804 - 2815
a
7.108 ± 0.004 Å
b
11.354 ± 0.006 Å
c
16.593 ± 0.009 Å
α
82.904 ± 0.008°
β
84.495 ± 0.008°
γ
72.746 ± 0.008°
Cell volume
1266.6 ± 1.2 Å3
Cell temperature
293 ± 2 K
Ambient diffraction temperature
293 ± 2 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.165
Residual factor for significantly intense reflections
0.0723
Weighted residual factors for significantly intense reflections
0.154
Weighted residual factors for all reflections included in the refinement
0.1884
Goodness-of-fit parameter for all reflections included in the refinement
