Information card for entry 7024708

Structure parameters

• Formula: C12 H28 N P2 Se2 Tl
• Calculated formula: C12 H28 N P2 Se2 Tl
• Title of publication: Thallium(I) complexes of dichalcogenido imidodiphosphinates {Tl[(EP(i)Pr(2))(2)N]}(n) (E = Te, Se, S): Synthesis, NMR spectra and a structural comparison.
• Authors of publication: Ritch, Jamie S.; Chivers, Tristram
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 7
• Pages of publication: 1745 - 1750
• a: 9.2446 ± 0.0018 Å
• b: 14.268 ± 0.003 Å
• c: 14.924 ± 0.003 Å
• α: 80.12 ± 0.03°
• β: 81.47 ± 0.03°
• γ: 84.22 ± 0.03°
• Cell volume: 1912.1 ± 0.7 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0485
• Residual factor for significantly intense reflections: 0.0372
• Weighted residual factors for significantly intense reflections: 0.0854
• Weighted residual factors for all reflections included in the refinement: 0.0925
• Goodness-of-fit parameter for all reflections included in the refinement: 1.084
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No