Crystallography Open Database

Information card for entry 7024725

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Structure parameters

Formula	C69 H103 B2 Cu La N14 O4
Calculated formula	C69 H103 B2 Cu La N14 O4
Title of publication	Soluble monometallic salen complexes derived from O-functionalised diamines as metalloligands for the synthesis of heterobimetallic complexes.
Authors of publication	Schley, Michael; Fritzsche, Sebastian; Lönnecke, Peter; Hey-Hawkins, Evamarie
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2010
Journal volume	39
Journal issue	17
Pages of publication	4090 - 4106
a	14.4518 ± 0.0008 Å
b	16.653 ± 0.0019 Å
c	17.2355 ± 0.0016 Å
α	108.151 ± 0.009°
β	109.351 ± 0.007°
γ	95.541 ± 0.007°
Cell volume	3625.4 ± 0.7 Å³
Cell temperature	130 ± 2 K
Ambient diffraction temperature	130 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0448
Residual factor for significantly intense reflections	0.033
Weighted residual factors for significantly intense reflections	0.0779
Weighted residual factors for all reflections included in the refinement	0.0847
Goodness-of-fit parameter for all reflections included in the refinement	1.035
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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