Information card for entry 7024774

Structure parameters

• Formula: C18 H24 N2 Ni0.5 P2
• Calculated formula: C18 H24 N2 Ni0.5 P2
• Title of publication: Reduction of oxygen catalyzed by nickel diphosphine complexes with positioned pendant amines.
• Authors of publication: Yang, Jenny Y.; Bullock, R. Morris; Dougherty, William G.; Kassel, W. Scott; Twamley, Brendan; DuBois, Daniel L.; Rakowski DuBois, M.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 12
• Pages of publication: 3001 - 3010
• a: 9.7763 ± 0.0002 Å
• b: 19.7795 ± 0.0004 Å
• c: 19.0291 ± 0.0003 Å
• α: 90°
• β: 101.121 ± 0.001°
• γ: 90°
• Cell volume: 3610.57 ± 0.12 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0317
• Residual factor for significantly intense reflections: 0.0297
• Weighted residual factors for significantly intense reflections: 0.0787
• Weighted residual factors for all reflections included in the refinement: 0.0804
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No