Information card for entry 7024776

Structure parameters

• Formula: H274 Na18 Ni6 O284 P6 W39
• Calculated formula: Na16 Ni6 O194.5 P6 W39
• Title of publication: Two hexa-TM-containing (TM = Co2+ and Ni2+) {P2W12}-based trimeric tungstophosphates.
• Authors of publication: Yao, Shuang; Zhang, Zhiming; Li, Yangguang; Wang, Enbo
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 16
• Pages of publication: 3884 - 3889
• a: 21.643 ± 0.006 Å
• b: 31.87 ± 0.006 Å
• c: 33.861 ± 0.007 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 23356 ± 9 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 63
• Hermann-Mauguin space group symbol: C m c m
• Hall space group symbol: -C 2c 2
• Residual factor for all reflections: 0.1307
• Residual factor for significantly intense reflections: 0.0619
• Weighted residual factors for significantly intense reflections: 0.1378
• Weighted residual factors for all reflections included in the refinement: 0.1758
• Goodness-of-fit parameter for all reflections included in the refinement: 1.009
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No