Information card for entry 7024798

Structure parameters

• Formula: C75 H185 Si24 Sn10
• Calculated formula: C75 H185 Si24 Sn10
• Title of publication: The formation of a metalloid Sn(10)[Si(SiMe(3))(3)](6) cluster compound and its relation to the alpha<‒>beta tin phase transition.
• Authors of publication: Schrenk, Claudio; Schellenberg, Inga; Pöttgen, Rainer; Schnepf, Andreas
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 7
• Pages of publication: 1872 - 1876
• a: 18.996 ± 0.004 Å
• b: 19.115 ± 0.004 Å
• c: 19.318 ± 0.004 Å
• α: 99.29 ± 0.03°
• β: 97.33 ± 0.03°
• γ: 102.66 ± 0.03°
• Cell volume: 6657 ± 3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0528
• Residual factor for significantly intense reflections: 0.0398
• Weighted residual factors for significantly intense reflections: 0.0946
• Weighted residual factors for all reflections included in the refinement: 0.0994
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No