Information card for entry 7024823

Structure parameters

• Formula: C73 H66 Ag Cl N2 O
• Calculated formula: C73 H66 Ag Cl N2 O
• Title of publication: IPr* an easily accessible highly hindered N-heterocyclic carbene.
• Authors of publication: Berthon-Gelloz, Guillaume; Siegler, Maxime A.; Spek, Anthony L.; Tinant, Bernard; Reek, Joost N. H.; Markó, István E
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 6
• Pages of publication: 1444 - 1446
• a: 12.331 ± 0.004 Å
• b: 19.066 ± 0.005 Å
• c: 24.981 ± 0.006 Å
• α: 90°
• β: 94.84 ± 0.02°
• γ: 90°
• Cell volume: 5852 ± 3 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0492
• Residual factor for significantly intense reflections: 0.0406
• Weighted residual factors for significantly intense reflections: 0.1045
• Weighted residual factors for all reflections included in the refinement: 0.1106
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No