Information card for entry 7024899

Structure parameters

• Formula: C82 H74 B N2 O P2 Zn
• Calculated formula: C82 H74 B N2 O P2 Zn
• Title of publication: Cationic organozinc complexes of a bis(phosphinimine) pincer ligand: synthesis, structural and polymerization studies.
• Authors of publication: Wheaton, Craig A.; Hayes, Paul G.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 16
• Pages of publication: 3861 - 3869
• a: 11.4348 ± 0.001 Å
• b: 15.8183 ± 0.0014 Å
• c: 19.2062 ± 0.0017 Å
• α: 86.685 ± 0.001°
• β: 75.823 ± 0.001°
• γ: 82.763 ± 0.001°
• Cell volume: 3340 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1351
• Residual factor for significantly intense reflections: 0.0662
• Weighted residual factors for significantly intense reflections: 0.1554
• Weighted residual factors for all reflections included in the refinement: 0.1883
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No