Crystallography Open Database

Information card for entry 7024954

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Structure parameters

Formula	C48 H82 N8 O9 S4
Calculated formula	C48 H82 N8 O9 S4
Title of publication	Synthesis, structure and chiroptical study of chiral macrocyclic imine nickel(II) coordination compounds derived from camphor.
Authors of publication	Wu, Tao; Li, Cheng-Hui; Li, Yi-Zhi; Zhang, Zhao-Gui; You, Xiao-Zeng
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2010
Journal volume	39
Journal issue	13
Pages of publication	3227 - 3232
a	8.9463 ± 0.0011 Å
b	28.733 ± 0.003 Å
c	11.133 ± 0.0012 Å
α	90°
β	90.905 ± 0.002°
γ	90°
Cell volume	2861.4 ± 0.6 Å³
Cell temperature	291 ± 2 K
Ambient diffraction temperature	291 ± 2 K
Number of distinct elements	5
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0378
Residual factor for significantly intense reflections	0.0344
Weighted residual factors for significantly intense reflections	0.0782
Weighted residual factors for all reflections included in the refinement	0.0791
Goodness-of-fit parameter for all reflections included in the refinement	1.048
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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