Information card for entry 7024959

Structure parameters

• Formula: C48 H88 Ag4 N4 O16 P8 S8
• Calculated formula: C48 H88 Ag4 N4 O16 P8 S8
• Title of publication: Construction of a monoanionic S,N,S-pincer ligand with a pyrrole core by sequential [1,2] phospho-Fries rearrangement. Characterization of palladium and silver coordination complexes.
• Authors of publication: Fraix, Aurore; Lutz, Martin; Spek, Anthony L.; Klein Gebbink, Robertus J. M.; van Koten, Gerard; Salaün, Jean-Yves; Jaffrès, Paul-Alain
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 11
• Pages of publication: 2942 - 2946
• a: 11.1886 ± 0.0004 Å
• b: 12.7764 ± 0.0006 Å
• c: 14.3823 ± 0.0007 Å
• α: 78.72 ± 0.002°
• β: 81.848 ± 0.002°
• γ: 72.571 ± 0.002°
• Cell volume: 1916.05 ± 0.15 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0366
• Residual factor for significantly intense reflections: 0.0243
• Weighted residual factors for significantly intense reflections: 0.0531
• Weighted residual factors for all reflections included in the refinement: 0.0568
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No