Information card for entry 7024980

Structure parameters

• Formula: C30 H41 N2 O P
• Calculated formula: C30 H41 N2 O P
• Title of publication: Planar-chiral imidazole-based phosphine ligands derived from [2.2]paracyclophane
• Authors of publication: Seacome, Richard J.; Coles, Martyn P.; Glover, Jean E.; Hitchcock, Peter B.; Rowlands, Gareth J.
• Journal of publication: Dalton Transactions
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 15
• Pages of publication: 3687
• a: 9.1186 ± 0.0003 Å
• b: 11.6152 ± 0.0003 Å
• c: 13.9871 ± 0.0004 Å
• α: 105.127 ± 0.001°
• β: 105.574 ± 0.002°
• γ: 102.542 ± 0.002°
• Cell volume: 1310.24 ± 0.07 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0686
• Residual factor for significantly intense reflections: 0.0543
• Weighted residual factors for significantly intense reflections: 0.1426
• Weighted residual factors for all reflections included in the refinement: 0.1532
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No