Information card for entry 7025014

Structure parameters

• Formula: C65 H101 I2 N4 O Sm2
• Calculated formula: C65 H101 I2 N4 O Sm2
• Title of publication: Low coordinate lanthanide(II) complexes supported by bulky guanidinato and amidinato ligands.
• Authors of publication: Heitmann, Dennis; Jones, Cameron; Mills, David P.; Stasch, Andreas
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 7
• Pages of publication: 1877 - 1882
• a: 16.84 ± 0.003 Å
• b: 10.807 ± 0.002 Å
• c: 37.239 ± 0.007 Å
• α: 90°
• β: 97.64 ± 0.03°
• γ: 90°
• Cell volume: 6717 ± 2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0671
• Residual factor for significantly intense reflections: 0.0433
• Weighted residual factors for significantly intense reflections: 0.075
• Weighted residual factors for all reflections included in the refinement: 0.0815
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No