High nuclearity manganese(iii) compounds containing phenol-pyrazole ligands: the influence of the ligand on the core geometry
Authors of publication
Viciano-Chumillas, Marta; de Ruiter, Graham; Tanase, Stefania; Smits, Jan M. M.; de Gelder, René; Mutikainen, Ilpo; Turpeinen, Urho; de Jongh, L. Jos; Reedijk, Jan
Journal of publication
Dalton Transactions
Year of publication
2010
Journal volume
39
Journal issue
20
Pages of publication
4991
a
15.284 ± 0.003 Å
b
15.918 ± 0.003 Å
c
18.924 ± 0.003 Å
α
82.82 ± 0.03°
β
69.5 ± 0.03°
γ
84.94 ± 0.03°
Cell volume
4273.8 ± 1.6 Å3
Cell temperature
173 ± 2 K
Ambient diffraction temperature
173 ± 2 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0935
Residual factor for significantly intense reflections
0.0463
Weighted residual factors for significantly intense reflections
0.0848
Weighted residual factors for all reflections included in the refinement
0.1011
Goodness-of-fit parameter for all reflections included in the refinement
