Information card for entry 7025074

Structure parameters

• Formula: C25 H42 Cl4 P2 Pd
• Calculated formula: C25 H41 Cl4 P2 Pd
• Title of publication: Coordination chemistry of cis,cis and trans,trans 1,1'-[1,2-phenylenebis(methylene)]bis(2,2,3,4,4-pentamethylphosphetane).
• Authors of publication: Coleman, Dennis; Edwards, Peter G.; Kariuki, Benson M.; Newman, Paul D.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 16
• Pages of publication: 3842 - 3850
• a: 8.7866 ± 0.0001 Å
• b: 10.8661 ± 0.0002 Å
• c: 15.9424 ± 0.0003 Å
• α: 109.667 ± 0.0008°
• β: 93.1967 ± 0.0008°
• γ: 95.8861 ± 0.001°
• Cell volume: 1419.13 ± 0.04 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0458
• Residual factor for significantly intense reflections: 0.0348
• Weighted residual factors for significantly intense reflections: 0.0741
• Weighted residual factors for all reflections included in the refinement: 0.0785
• Goodness-of-fit parameter for all reflections included in the refinement: 1.007
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No