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Information card for entry 7025178
Preview
Coordinates | 7025178.cif |
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Original paper (by DOI) | HTML |
Formula | C68 H77 N7 O4 Zn2 |
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Calculated formula | C68 H77 N7 O4 Zn2 |
Title of publication | Self-assembly of Zn(salphen) complexes: steric regulation, stability studies and crystallographic analysis revealing an unexpected dimeric 3,3'-t-Bu-substituted Zn(salphen) complex. |
Authors of publication | Martínez Belmonte, Marta; Wezenberg, Sander J.; Haak, Robert M.; Anselmo, Daniele; Escudero-Adán, Eduardo C; Benet-Buchholz, Jordi; Kleij, Arjan W. |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2010 |
Journal volume | 39 |
Journal issue | 19 |
Pages of publication | 4541 - 4550 |
a | 16.3096 ± 0.0006 Å |
b | 13.0108 ± 0.0005 Å |
c | 29.4617 ± 0.0011 Å |
α | 90° |
β | 102.979 ± 0.002° |
γ | 90° |
Cell volume | 6092.1 ± 0.4 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.1004 |
Residual factor for significantly intense reflections | 0.0828 |
Weighted residual factors for significantly intense reflections | 0.2053 |
Weighted residual factors for all reflections included in the refinement | 0.2173 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.051 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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