Information card for entry 7025184

Structure parameters

• Formula: C16 H22 Al Cl3 N P Si
• Calculated formula: C16 H22 Al Cl3 N P Si
• SMILES: [Al]([N](=P(C)(c1ccccc1)c1ccccc1)[Si](C)(C)C)(Cl)(Cl)Cl
• Title of publication: Reactivity of Zn(II), Mg(II) and Al(III) chlorides with a phosphinimine ligand: new tetrameric inverse crown ether structures.
• Authors of publication: Valerio Cárdenas, Cintya; Muñoz Hernández, Miguel Angel; Grévy, Jean-Michel
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 28
• Pages of publication: 6441 - 6448
• a: 9.7388 ± 0.0013 Å
• b: 14.3203 ± 0.0019 Å
• c: 14.5442 ± 0.0019 Å
• α: 90°
• β: 94.085 ± 0.004°
• γ: 90°
• Cell volume: 2023.2 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0422
• Residual factor for significantly intense reflections: 0.0387
• Weighted residual factors for significantly intense reflections: 0.1087
• Weighted residual factors for all reflections included in the refinement: 0.111
• Goodness-of-fit parameter for all reflections included in the refinement: 1.069
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No