Information card for entry 7025199

Structure parameters

• Chemical name: (N,N,N',N'-tetramethylenediamine)-chloro-pentafluorophenyl-palladium(II)
• Formula: C12 H16 Cl F5 N2 Pd
• Calculated formula: C12 H16 Cl F5 N2 Pd
• Title of publication: Palladium(II) complexes with pentafluorophenyl ligands: structures, C6F5 fluxionality by 2D-NMR studies and pre-catalysts for the vinyl addition polymerization of norbornene.
• Authors of publication: Blank, Frederik; Scherer, Harald; Ruiz, José; Rodríguez, Venancio; Janiak, Christoph
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 15
• Pages of publication: 3609 - 3619
• a: 12.545 ± 0.0007 Å
• b: 19.9097 ± 0.0008 Å
• c: 11.9976 ± 0.0008 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2996.6 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 41
• Hermann-Mauguin space group symbol: A b a 2
• Hall space group symbol: A 2 -2ab
• Residual factor for all reflections: 0.0344
• Residual factor for significantly intense reflections: 0.0326
• Weighted residual factors for significantly intense reflections: 0.0753
• Weighted residual factors for all reflections included in the refinement: 0.0763
• Goodness-of-fit parameter for all reflections included in the refinement: 1.081
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No