Information card for entry 7025240

Structure parameters

• Formula: C40 H66 N4 O2 Si4 Y2
• Calculated formula: C40 H66 N4 O2 Si4 Y2
• Title of publication: The behavior of pyrrolyl ligands within the rare-earth metal alkyl complexes. Insertion of C=N and C=O double bonds into Ln-sigma-C bonds.
• Authors of publication: Yang, Yi; Cui, Dongmei; Chen, Xuesi
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 16
• Pages of publication: 3959 - 3967
• a: 11.3031 ± 0.0009 Å
• b: 37.091 ± 0.003 Å
• c: 12.1407 ± 0.001 Å
• α: 90°
• β: 91.727 ± 0.001°
• γ: 90°
• Cell volume: 5087.6 ± 0.7 ų
• Cell temperature: 187 ± 2 K
• Ambient diffraction temperature: 187 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0877
• Residual factor for significantly intense reflections: 0.0507
• Weighted residual factors for significantly intense reflections: 0.1296
• Weighted residual factors for all reflections included in the refinement: 0.1485
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No