Information card for entry 7025272

Structure parameters

• Common name: ((CH3)(dppz)(pyridine)palladium(ii))SbF6
• Formula: C24 H18 F6 N5 Pd Sb
• Calculated formula: C24 H18 F6 N5 Pd Sb
• SMILES: [Sb](F)(F)(F)(F)(F)[F-].[Pd]1([n]2cccc3c2c2[n]1cccc2c1nc2c(nc31)cccc2)([n]1ccccc1)C
• Title of publication: Tuning the electronic properties of dppz-ligands and their palladium(II) complexes.
• Authors of publication: Butsch, Katharina; Gust, Ronald; Klein, Axel; Ott, Ingo; Romanski, Marco
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 18
• Pages of publication: 4331 - 4340
• a: 9.1171 ± 0.0016 Å
• b: 10.1421 ± 0.002 Å
• c: 16.5134 ± 0.0031 Å
• α: 82.022 ± 0.015°
• β: 80.729 ± 0.015°
• γ: 68.043 ± 0.014°
• Cell volume: 1392.5 ± 0.5 ų
• Cell temperature: 170 ± 2 K
• Ambient diffraction temperature: 170 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1264
• Residual factor for significantly intense reflections: 0.0477
• Weighted residual factors for significantly intense reflections: 0.0918
• Weighted residual factors for all reflections included in the refinement: 0.1088
• Goodness-of-fit parameter for all reflections included in the refinement: 0.734
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No