Information card for entry 7025297

Structure parameters

• Formula: C69.5 H61.5 N3.5 O0.5 P4 S4 U
• Calculated formula: C70 H59 N3 O0.5 P4 S4 U
• Title of publication: Easy access to uranium nucleophilic carbene complexes.
• Authors of publication: Tourneux, Jean-Christophe; Berthet, Jean-Claude; Thuéry, Pierre; Mézailles, Nicolas; Le Floch, Pascal; Ephritikhine, Michel
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 10
• Pages of publication: 2494 - 2496
• a: 13.8488 ± 0.0004 Å
• b: 28.6755 ± 0.0015 Å
• c: 17.9735 ± 0.001 Å
• α: 90°
• β: 96.481 ± 0.003°
• γ: 90°
• Cell volume: 7092 ± 0.6 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0915
• Residual factor for significantly intense reflections: 0.061
• Weighted residual factors for significantly intense reflections: 0.1538
• Weighted residual factors for all reflections included in the refinement: 0.1624
• Goodness-of-fit parameter for all reflections included in the refinement: 1.05
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No