Information card for entry 7025300

Structure parameters

• Formula: C41 H20 B F24 N4 O2 Rh
• Calculated formula: C41 H20 B F24 N4 O2 Rh
• Title of publication: Highly efficient Rh(I) and Ir(I) single and dual metal catalysed dihydroalkoxylation reactions of alkyne diols.
• Authors of publication: Ho, Joanne Hui Hui; Hodgson, Richard; Wagler, Jörg; Messerle, Barbara Ann
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 17
• Pages of publication: 4062 - 4069
• a: 10.3971 ± 0.0001 Å
• b: 14.9619 ± 0.0002 Å
• c: 15.1133 ± 0.0002 Å
• α: 92.045 ± 0.001°
• β: 105.259 ± 0.001°
• γ: 98.587 ± 0.001°
• Cell volume: 2235.78 ± 0.05 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0549
• Residual factor for significantly intense reflections: 0.0447
• Weighted residual factors for significantly intense reflections: 0.1086
• Weighted residual factors for all reflections included in the refinement: 0.1132
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No