The gas-phase structure of octaphenyloctasilsesquioxane Si8O12Ph8 and the crystal structures of Si8O12(p-tolyl)8 and Si8O12(p-ClCH2C6H4)8.
Authors of publication
Zakharov, Alexander V.; Masters, Sarah L.; Wann, Derek A.; Shlykov, Sergei A.; Girichev, Georgiy V.; Arrowsmith, Sophie; Cordes, David B.; Lickiss, Paul D.; White, Andrew J. P.
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2010
Journal volume
39
Journal issue
30
Pages of publication
6960 - 6966
a
12.8106 ± 0.0006 Å
b
13.2923 ± 0.0006 Å
c
22.1442 ± 0.001 Å
α
76.315 ± 0.004°
β
75.028 ± 0.004°
γ
61.699 ± 0.005°
Cell volume
3178.3 ± 0.3 Å3
Cell temperature
173 ± 2 K
Ambient diffraction temperature
173 ± 2 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.1331
Residual factor for significantly intense reflections
0.0547
Weighted residual factors for significantly intense reflections
0.1235
Weighted residual factors for all reflections included in the refinement
0.1349
Goodness-of-fit parameter for all reflections included in the refinement
