Information card for entry 7025478

Structure parameters

• Common name: Bis(tris(trimethylsilyl)germyl)plumbylene
• Chemical name: Bis[tris(trimethylsilyl)germyl]plumbylene
• Formula: C18 H54 Ge2 Pb Si6
• Calculated formula: C18 H54 Ge2 Pb Si6
• Title of publication: EPR spectroscopic characterization of persistent germyl-substituted Pb(III)- and Sn(III)-radicals.
• Authors of publication: Kurzbach, Dennis; Yao, Shenglai; Hinderberger, Dariush; Klinkhammer, Karl W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 28
• Pages of publication: 6449 - 6459
• a: 16.275 ± 0.003 Å
• b: 22.189 ± 0.004 Å
• c: 22.437 ± 0.005 Å
• α: 110.5 ± 0.03°
• β: 100.71 ± 0.03°
• γ: 100.26 ± 0.03°
• Cell volume: 7192 ± 3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1666
• Residual factor for significantly intense reflections: 0.0812
• Weighted residual factors for significantly intense reflections: 0.1702
• Weighted residual factors for all reflections included in the refinement: 0.2021
• Goodness-of-fit parameter for all reflections included in the refinement: 1.161
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No