Information card for entry 7025482

Structure parameters

• Formula: C43 H121 Ge K O4 Pb Si11
• Calculated formula: C43 H121 Ge1.4565 K O4 Pb Si10.54
• Title of publication: EPR spectroscopic characterization of persistent germyl-substituted Pb(III)- and Sn(III)-radicals.
• Authors of publication: Kurzbach, Dennis; Yao, Shenglai; Hinderberger, Dariush; Klinkhammer, Karl W.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 28
• Pages of publication: 6449 - 6459
• a: 12.223 ± 0.002 Å
• b: 24.446 ± 0.004 Å
• c: 24.96 ± 0.004 Å
• α: 90°
• β: 99.962 ± 0.005°
• γ: 90°
• Cell volume: 7346 ± 2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0852
• Residual factor for significantly intense reflections: 0.0455
• Weighted residual factors for significantly intense reflections: 0.0886
• Weighted residual factors for all reflections included in the refinement: 0.0991
• Goodness-of-fit parameter for all reflections included in the refinement: 1.189
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No