Information card for entry 7025631

Structure parameters

• Formula: C20 H24 Cl2 Ge N2
• Calculated formula: C20 H24 Cl2 Ge N2
• SMILES: c1(c(cc(cc1C)C)C)N1C=CN([Ge]1(Cl)Cl)c1c(cc(cc1C)C)C
• Title of publication: Facile synthesis of dichlorosilane by metathesis reaction and dehydrogenation of dihydrogermane by a frustrated Lewis pair.
• Authors of publication: Jana, Anukul; Tavcar, Gasper; Roesky, Herbert W.; Schulzke, Carola
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 27
• Pages of publication: 6217 - 6220
• a: 17.174 ± 0.003 Å
• b: 7.3558 ± 0.0015 Å
• c: 15.804 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1996.5 ± 0.7 ų
• Cell temperature: 140 ± 2 K
• Ambient diffraction temperature: 140 ± 2 K
• Number of distinct elements: 5
• Space group number: 60
• Hermann-Mauguin space group symbol: P b c n
• Hall space group symbol: -P 2n 2ab
• Residual factor for all reflections: 0.0697
• Residual factor for significantly intense reflections: 0.0403
• Weighted residual factors for significantly intense reflections: 0.0642
• Weighted residual factors for all reflections included in the refinement: 0.0702
• Goodness-of-fit parameter for all reflections included in the refinement: 1.101
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No