Information card for entry 7025668

Structure parameters

• Formula: Fe6 H140 K2 Na22 O247 P6 W48
• Calculated formula: Fe6 K2 Na4.2 O218.6 P6 W48
• Title of publication: Understanding and mapping the assembly of a family of trimeric polyoxometalates: transition metal mediated Wells-Dawson (M18)-trimers.
• Authors of publication: Boyd, Thomas; Mitchell, Scott G.; Miras, Haralampos N.; Long, De-Liang; Cronin, Leroy
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 28
• Pages of publication: 6460 - 6465
• a: 17.5835 ± 0.0005 Å
• b: 20.6617 ± 0.0003 Å
• c: 36.5786 ± 0.0007 Å
• α: 89.811 ± 0.001°
• β: 82.173 ± 0.002°
• γ: 75.046 ± 0.002°
• Cell volume: 12712.5 ± 0.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1702
• Residual factor for significantly intense reflections: 0.0676
• Weighted residual factors for significantly intense reflections: 0.1579
• Weighted residual factors for all reflections included in the refinement: 0.1785
• Goodness-of-fit parameter for all reflections included in the refinement: 0.816
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No