Information card for entry 7025896

Structure parameters

• Formula: C113 H146 B4 Cl2 F24 N32 P4 Rh8
• Calculated formula: C113 H146 B4 Cl2 F24 N32 P4 Rh8
• Title of publication: Homo- and heterodinuclear complexes of the tetrakis(pyrazolyl)borate ligand.
• Authors of publication: Hallett, Andrew J.; Adams, Christopher J.; Anderson, Kirsty M.; Baber, R. Angharad; Connelly, Neil G.; Prime, Christopher J.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 25
• Pages of publication: 5899 - 5907
• a: 28.003 ± 0.007 Å
• b: 13.173 ± 0.003 Å
• c: 17.633 ± 0.004 Å
• α: 90°
• β: 99.475 ± 0.016°
• γ: 90°
• Cell volume: 6416 ± 3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 8
• Space group number: 5
• Hermann-Mauguin space group symbol: C 1 2 1
• Hall space group symbol: C 2y
• Residual factor for all reflections: 0.0259
• Residual factor for significantly intense reflections: 0.0235
• Weighted residual factors for significantly intense reflections: 0.0547
• Weighted residual factors for all reflections included in the refinement: 0.0553
• Goodness-of-fit parameter for all reflections included in the refinement: 0.985
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No