Information card for entry 7025899

Structure parameters

• Formula: C53 H48 B Cl6 F6 N8 O2 P3 Rh2
• Calculated formula: C53 H48 B Cl6 F6 N8 O2 P3 Rh2
• Title of publication: Homo- and heterodinuclear complexes of the tetrakis(pyrazolyl)borate ligand.
• Authors of publication: Hallett, Andrew J.; Adams, Christopher J.; Anderson, Kirsty M.; Baber, R. Angharad; Connelly, Neil G.; Prime, Christopher J.
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 25
• Pages of publication: 5899 - 5907
• a: 13.281 ± 0.003 Å
• b: 13.38 ± 0.003 Å
• c: 17.393 ± 0.003 Å
• α: 84.36 ± 0.02°
• β: 74.524 ± 0.016°
• γ: 84.84 ± 0.03°
• Cell volume: 2957.7 ± 1.1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0562
• Residual factor for significantly intense reflections: 0.0487
• Weighted residual factors for significantly intense reflections: 0.1163
• Weighted residual factors for all reflections included in the refinement: 0.1204
• Goodness-of-fit parameter for all reflections included in the refinement: 1.062
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No