Information card for entry 7025916

Structure parameters

• Formula: C16 H36 Cl2 Ru S4
• Calculated formula: C16 H36 Cl2 Ru S4
• Title of publication: A straightforward and generalizable synthetic methodology for the synthesis of ruthenium(II) complexes with thioether ligands from either Ru(III) or Ru(0) precursors.
• Authors of publication: Maiti, Biplab K.; Görls, Helmar; Klobes, Olaf; Imhof, Wolfgang
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 24
• Pages of publication: 5713 - 5720
• a: 20.6376 ± 0.0009 Å
• b: 20.1958 ± 0.0009 Å
• c: 11.2202 ± 0.0003 Å
• α: 90°
• β: 98.911 ± 0.003°
• γ: 90°
• Cell volume: 4620.1 ± 0.3 ų
• Cell temperature: 183 ± 2 K
• Ambient diffraction temperature: 183 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0843
• Residual factor for significantly intense reflections: 0.0418
• Weighted residual factors for significantly intense reflections: 0.0889
• Weighted residual factors for all reflections included in the refinement: 0.1052
• Goodness-of-fit parameter for all reflections included in the refinement: 0.987
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No