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Information card for entry 7026068
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Coordinates | 7026068.cif |
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Original paper (by DOI) | HTML |
Common name | 1-Dicyclohexylphosphino-1,2,2-tris(2',4',6'- triisopropylphenyl)disilene |
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Chemical name | 1-Dicyclohexylphosphino-1,2,2-tris(2',4',6'-triisopropylphenyl)disilene |
Formula | C57 H91 P Si2 |
Calculated formula | C57 H91 P Si2 |
Title of publication | Synthesis, characterisation and complexation of phosphino disilenes. |
Authors of publication | Hartmann, Marco; Haji-Abdi, Abdishakur; Abersfelder, Kai; Haycock, Peter R.; White, Andrew J. P.; Scheschkewitz, David |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2010 |
Journal volume | 39 |
Journal issue | 39 |
Pages of publication | 9288 - 9295 |
a | 20.8212 ± 0.0012 Å |
b | 10.5035 ± 0.0006 Å |
c | 26.2637 ± 0.0016 Å |
α | 90° |
β | 103.603 ± 0.001° |
γ | 90° |
Cell volume | 5582.6 ± 0.6 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 4 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0874 |
Residual factor for significantly intense reflections | 0.0839 |
Weighted residual factors for significantly intense reflections | 0.1677 |
Weighted residual factors for all reflections included in the refinement | 0.1694 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.283 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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