Information card for entry 7026071

Structure parameters

• Formula: C78 H119 P2 Pd Si2
• Calculated formula: C78 H119 P2 Pd Si2
• Title of publication: Synthesis, characterisation and complexation of phosphino disilenes.
• Authors of publication: Hartmann, Marco; Haji-Abdi, Abdishakur; Abersfelder, Kai; Haycock, Peter R.; White, Andrew J. P.; Scheschkewitz, David
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 39
• Pages of publication: 9288 - 9295
• a: 19.87013 ± 0.00007 Å
• b: 14.06651 ± 0.00004 Å
• c: 27.06129 ± 0.00008 Å
• α: 90°
• β: 100.968 ± 0.0003°
• γ: 90°
• Cell volume: 7425.55 ± 0.04 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.029
• Residual factor for significantly intense reflections: 0.0268
• Weighted residual factors for significantly intense reflections: 0.0704
• Weighted residual factors for all reflections included in the refinement: 0.0714
• Goodness-of-fit parameter for all reflections included in the refinement: 1.061
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No