Information card for entry 7026381

Structure parameters

• Formula: C10 H30 N4 O8 Pd
• Calculated formula: C10 H30 N4 O8 Pd
• Title of publication: Syntheses, solid state and solution structures of the palladium(II) complexes of malonamide-derived open-chain and macrocyclic ligands.
• Authors of publication: Gavrish, Sergey P.; Lampeka, Yaroslaw D.; Pritzkow, Hans; Lightfoot, Philip
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 33
• Pages of publication: 7706 - 7713
• a: 7.256 ± 0.0002 Å
• b: 24.9406 ± 0.0006 Å
• c: 9.5763 ± 0.0002 Å
• α: 90°
• β: 92.208 ± 0.002°
• γ: 90°
• Cell volume: 1731.73 ± 0.07 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0262
• Residual factor for significantly intense reflections: 0.0242
• Weighted residual factors for significantly intense reflections: 0.0615
• Weighted residual factors for all reflections included in the refinement: 0.0627
• Goodness-of-fit parameter for all reflections included in the refinement: 1.087
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No