Information card for entry 7026643

Structure parameters

• Formula: C40 H40 Cl2 O8 Pd2 Se4
• Calculated formula: C40 H40 Cl2 O8 Pd2 Se4
• Title of publication: Tetradentate selenium ligand as a building block for homodinuclear complexes of Pd(II) and Ru(II) having seven membered rings or bis-pincer coordination mode: high catalytic activity of Pd-complexes for Heck reaction.
• Authors of publication: Das, Dipanwita; Singh, Pradhumn; Singh, Monika; Singh, Ajai Kumar
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 45
• Pages of publication: 10876 - 10882
• a: 11.026 ± 0.005 Å
• b: 14.321 ± 0.006 Å
• c: 15.336 ± 0.007 Å
• α: 91.562 ± 0.007°
• β: 104.662 ± 0.005°
• γ: 96.774 ± 0.007°
• Cell volume: 2322.3 ± 1.8 ų
• Cell temperature: 273 ± 2 K
• Ambient diffraction temperature: 273 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1073
• Residual factor for significantly intense reflections: 0.0613
• Weighted residual factors for significantly intense reflections: 0.141
• Weighted residual factors for all reflections included in the refinement: 0.16
• Goodness-of-fit parameter for all reflections included in the refinement: 1.294
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No