Information card for entry 7026732

Structure parameters

• Formula: C8 H9 Br Cl2 N O V
• Calculated formula: C8 H9 Br Cl2 N O V
• Title of publication: Synthesis of (arylimido)vanadium complexes and their application for oxidative coupling reactions of silyl enol ether derivatives.
• Authors of publication: Nishina, Masafumi; Moriuchi, Toshiyuki; Hirao, Toshikazu
• Journal of publication: Dalton transactions (Cambridge, England : 2003)
• Year of publication: 2010
• Journal volume: 39
• Journal issue: 41
• Pages of publication: 9936 - 9940
• a: 7.6595 ± 0.001 Å
• b: 11.7903 ± 0.0014 Å
• c: 13.1806 ± 0.0019 Å
• α: 90°
• β: 101.426 ± 0.004°
• γ: 90°
• Cell volume: 1166.7 ± 0.3 ų
• Cell temperature: 123.1 K
• Ambient diffraction temperature: 123 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/a 1
• Hall space group symbol: -P 2yab
• Residual factor for significantly intense reflections: 0.0484
• Weighted residual factors for all reflections included in the refinement: 0.1275
• Goodness-of-fit parameter for all reflections included in the refinement: 1.095
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No