Structural, MALDI-TOF-MS, magnetic and spectroscopic studies of new dinuclear copper(II), cobalt(II) and zinc(II) complexes containing a biomimicking μ-OH bridge.
Authors of publication
Núñez, Cristina; Bastida, Rufina; Macías, Alejandro; Valencia, Laura; Neuman, Nicolás I; Rizzi, Alberto C.; Brondino, Carlos D.; González, Pablo J; Capelo, José Luis; Lodeiro, Carlos
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2010
Journal volume
39
Journal issue
48
Pages of publication
11654 - 11663
a
10.711 ± 0.005 Å
b
12.273 ± 0.005 Å
c
16.182 ± 0.005 Å
α
67.947 ± 0.005°
β
86.665 ± 0.005°
γ
70.868 ± 0.005°
Cell volume
1857.6 ± 1.3 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
8
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0319
Residual factor for significantly intense reflections
0.0259
Weighted residual factors for significantly intense reflections
0.0641
Weighted residual factors for all reflections included in the refinement
0.0661
Goodness-of-fit parameter for all reflections included in the refinement
