Preparation and characterisation of divalent hard and soft metal (M = Ca, Co, Cu, Zn, Cd, Hg and Pb) complexes of 1,10-dithia-18-crown-6: structural versatility.
Authors of publication
Park, In-Hyeok; Park, Ki-Min; Lee, Shim Sung
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2010
Journal volume
39
Journal issue
40
Pages of publication
9696 - 9704
a
10.455 ± 0.002 Å
b
14.087 ± 0.003 Å
c
11.199 ± 0.003 Å
α
90°
β
106.144 ± 0.004°
γ
90°
Cell volume
1584.3 ± 0.6 Å3
Cell temperature
174 ± 2 K
Ambient diffraction temperature
174 ± 2 K
Number of distinct elements
6
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/n 1
Hall space group symbol
-P 2yn
Residual factor for all reflections
0.0404
Residual factor for significantly intense reflections
0.0332
Weighted residual factors for significantly intense reflections
0.0845
Weighted residual factors for all reflections included in the refinement
0.0893
Goodness-of-fit parameter for all reflections included in the refinement
