Preparation and characterisation of divalent hard and soft metal (M = Ca, Co, Cu, Zn, Cd, Hg and Pb) complexes of 1,10-dithia-18-crown-6: structural versatility.
Authors of publication
Park, In-Hyeok; Park, Ki-Min; Lee, Shim Sung
Journal of publication
Dalton transactions (Cambridge, England : 2003)
Year of publication
2010
Journal volume
39
Journal issue
40
Pages of publication
9696 - 9704
a
10.9492 ± 0.0012 Å
b
11.6596 ± 0.0013 Å
c
15.2396 ± 0.0018 Å
α
90°
β
90.114 ± 0.005°
γ
90°
Cell volume
1945.5 ± 0.4 Å3
Cell temperature
173 ± 2 K
Ambient diffraction temperature
173 ± 2 K
Number of distinct elements
6
Space group number
9
Hermann-Mauguin space group symbol
C 1 c 1
Hall space group symbol
C -2yc
Residual factor for all reflections
0.0406
Residual factor for significantly intense reflections
0.0392
Weighted residual factors for significantly intense reflections
0.0995
Weighted residual factors for all reflections included in the refinement
0.1008
Goodness-of-fit parameter for all reflections included in the refinement
